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A tower used in the fractionation of crude oil may have from 16 to 28 trays, but one used in the fractionation (superfractionation) of liquefied gases may have 30–100 trays. Towers concerned with the distillation of liquefied gases are only a few feet in diameter but may be up to 200 ft. Where c is the capacity in bbl/day, d is the diameter in feet, and r is the amount of residuum expressed as a fraction of the feedstock ( Parkash, 2003 Gary et al., 2007 Speight, 2014a, 2017 Hsu and Robinson, 2017).Ī tower stripping unwanted volatile material from gas oil may be only 3 or 4 ft. Thus there are internal flows of vapor and liquid within the column as well as external flows of feeds and product streams, into and out of the column.
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The condensed liquid that is removed from the system is known as the distillate or top product. Some of this liquid is recycled back to the top of the column and this is called the reflux. The condensed liquid is stored in a holding vessel known as the reflux drum. The vapor moves up the column, and as it exits the top of the unit, it is cooled by a condenser. The liquid removed from the reboiler is known as the bottoms. The vapor raised in the reboiler is reintroduced into the unit at the bottom of the column. In refineries the heating source may be the output streams of other columns. The source of heat input can be any suitable fluid, although in most chemical plants this is normally steam. Heat is supplied to the reboiler to generate vapor. The feed flows down the column where it is collected at the bottom in the reboiler. The feed tray divides the column into a top (enriching, rectification) section and a bottom (stripping) section. In a crude oil distillation unit the feedstock liquid mixture is introduced usually near the middle of the column to a tray known as the feed tray. Individual parts of an atmospheric distillation column. The rapid expansion of the water as it flashes to steam can create very damaging overpressures.įigure 4.5. Likewise, it is one of the principal applications of trip systems.Īnother quite different hazard in a distillation column is the ingress of water. The protection of distillation columns is one of the topics treated in detail in codes for pressure relief such as APIRP 521. Again pressure relief devices are required to provide protection. Deposition of flammable materials on packing surfaces has led to many fires on opening of distillation column for maintenance.Īnother hazard is overpressure due to heat radiation from fire.
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On columns operating at or near atmospheric pressure, full vacuum design, vacuum breakers, or inert gas injection is needed for protection. On the other hand, loss of steam at the reboiler can cause underpressure in the column. It is necessary to protect against this by higher pressure design, relief valves, or HIPS. If cooling at the condenser is lost, the column may suffer overpressure. A distillation column has a large input of heat at the reboiler and a large output at the condenser. The reduction of hazard in distillation columns by the limitation of inventory has been discussed above. The conditions of operation of the equipment associated with the distillation column, particularly the reboiler and bottoms pump, are severe, so that failure is more probable. There are a number of situations which may lead to loss of containment of this liquid.
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Minimize to tray keygen or key generator might contain a trojan horse opening a backdoor on your computer.In Lees' Loss Prevention in the Process Industries (Fourth Edition), 2012 11.8.4 Distillation Columnsĭistillation columns present a hazard in that they contain large inventories of flammable boiling liquid, usually under pressure. These infections might corrupt your computer installation or breach your privacy.
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